乙酸-[2-(4-辛基苯基)]乙酯合成路线 （共 6 条）
反应条件
triethylamine in methanol; water T=40°C; 2 h;
参考文献
SYNTHON BV; GIELING, Reinerus Gerardus
Patent: WO2012/41707 A1, 2012 ;
Location in patent: Page/Page column 12-13 ;
反应条件
1.1: lithium borohydride / tetrahydrofuran / 0.62 h / 0 °C / Inert atmosphere 1.2: pH < 6 2.1: triethylamine / water; methanol / 2 h / 40 °C View Scheme
参考文献
WO2012/41359 A1, ;
WO2012/41405 A1, ;
反应条件
1: pyridine / dichloromethane / 20 °C 2: triethylamine / 1,4-dioxane / 24 h / 70 °C 3: water / 1,4-dioxane / 16 h / 40 °C / pH ~ 9 - 10 View Scheme
反应条件
1: triethylamine / 1,4-dioxane / 24 h / 70 °C 2: water / 1,4-dioxane / 16 h / 40 °C / pH ~ 9 - 10 View Scheme
反应条件
1: With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal in methanol T=50°C; P=37503.8 Torr; 3.83333 h; 2: With sodium carbonate in water T=50 - 65°C;
参考文献
SYNTHON BV; GIELING, Reinerus Gerardus
Patent: WO2012/41707 A1, 2012 ;
Location in patent: Page/Page column 13-14 ;
反应条件
1: toluene-4-sulfonic acid / toluene / 0.5 h / 50 °C / Reflux 2: hydrogen / 5 palladium on charcoal / toluene / 2 h / 30 °C / 26252.6 Torr View Scheme
参考文献
SYNTHON B.V.; KRAJZOVIC, Jozef; GIELING, Reinerus Gerardus; DYMACEK, Bohumil
Patent: WO2012/41405 A1, 2012 ;
Title/Abstract Full Text Show Details
SYNTHON BV; GIELING, Reinerus Gerardus
Patent: WO2012/41707 A1, 2012 ;
