2-甲基-2-丙基2-吡啶基碳酸酯合成路线 （共 39 条）
反应条件
triethylamine in water; N,N-dimethyl-formamide 7 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 12 p. 3570 - 3575
反应条件
in acetonitrile T=25°C; Kinetics;
参考文献
Kim, Min-Young; Lee, Jae-In; Um, Ik-Hwan
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 4 p. 1115 - 1119
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
24 h; Ambient temperature;
参考文献
Kim, Sunggak; Lee, Jae In; Yi, Kyu Yang
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 12 p. 3570 - 3575
反应条件
pyridine in dichloromethane
5 h; Ambient temperature; Yield given;
参考文献
Kim, Sunggak; Lee, Jae In; Yi, Kyu Yang
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 12 p. 3570 - 3575
反应条件
1: pyridine / toluene; CH2Cl2 / 0.25 h / -10 - 0 °C
2: pyridine / CH2Cl2 / 5 h / Ambient temperature
View Scheme
参考文献
Kim, Sunggak; Lee, Jae In; Yi, Kyu Yang
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 12 p. 3570 - 3575
反应条件
1: (C2H5)3N / dimethylformamide; H2O / 6 h / Ambient temperature
2: pyridine / toluene; CH2Cl2 / 0.25 h / -10 - 0 °C
3: pyridine / CH2Cl2 / 5 h / Ambient temperature
View Scheme
参考文献
Kim, Sunggak; Lee, Jae In; Yi, Kyu Yang
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 12 p. 3570 - 3575
反应条件
pyridine
1.) CH2Cl2, 0 deg C, 0.5 h; 2.) CH2Cl2, r.t., 5 h; Yield given. Multistep reaction;
参考文献
Kim, Sunggak; Lee, Jae In
Chemistry Letters, 1984 , p. 237 - 238
反应条件
1) CH2Cl2, -35 deg C to r. t., 6 h, 2) THF, -35 deg C, 18 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Brodt, Werner
Chemische Berichte, 1985 , vol. 118, # 2 p. 468 - 482
反应条件
in dichloromethane
2 h; Ambient temperature;
参考文献
Kim, Sunggak; Lee, Jae In; Yi, Kyu Yang
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 12 p. 3570 - 3575
