(6Z)-3-甲基-4,5,8,9-四氢环辛四烯并[d][1,2]恶唑合成路线 （共 3 条）
反应条件
1: 96 percent / m-CPBA / CHCl3 / 0 °C
2: 96 percent / H5IO6 / H2O / 0.33 h / 85 °C / pH=7.1
View Scheme
参考文献
Williams, Peter D.; LeGoff, Eugene
Heterocycles, 1984 , vol. 22, # 2 p. 269 - 270
反应条件
1: 96 percent / m-CPBA / CHCl3 / 0 °C
2: 96 percent / H5IO6 / H2O / 0.33 h / 85 °C / pH=7.1
3: 97 percent / tetrahydrofuran / 12 h / 25 °C
View Scheme
参考文献
Williams, Peter D.; LeGoff, Eugene
Heterocycles, 1984 , vol. 22, # 2 p. 269 - 270
反应条件
1: 96 percent / m-CPBA / CHCl3 / 0 °C
2: 96 percent / H5IO6 / H2O / 0.33 h / 85 °C / pH=7.1
3: 97 percent / tetrahydrofuran / 12 h / 25 °C
4: 99 percent / H2, Et3N / 5percent Rh/C / ethanol / 30 h / 3040 Torr
View Scheme
参考文献
Williams, Peter D.; LeGoff, Eugene
Heterocycles, 1984 , vol. 22, # 2 p. 269 - 270
