1: With sodium hydroxide 2: With sodium acetate; acetic anhydride Further stages.;
参考文献
Obushak, Mykola D.; Pokhodylo, Nazariy T.; Ostapiuk, Yuri V.; Matiychuk, Vasyl S.
Phosphorus, Sulfur and Silicon and the Related Elements, 2008 , vol. 183, # 1 p. 136 - 143
1: glacial acetic acid; nitric acid / 15 °C / Man laesst dann die Temperatur des Gemisches auf 40-45gradC steigen und giesst schnell in Eiswasser. Man kann die beiden Aldehyde in Form der Natriumsalze, Bariumsalze oder durch NaHSO3 trennen. 2: sodium acetate View Scheme
参考文献
Taege
Chemische Berichte, 1887 , vol. 20, p. 2110
Archiv der Pharmazie (Weinheim, Germany), 1891 , vol. 229, p. 82
1: With iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=20°C; 2: With sodium thiosulfate in water; dimethyl sulfoxide 3: With ammonium chloride in water