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乙二醇
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63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-碘萘
合成路线
（共 431 条）
90-14-2
1-碘萘
+
107-13-1
丙烯腈
→
反应条件
70067-70-8
反应条件
chromium dichloride; ethylenediamine in N,N-dimethyl-formamide T=80°C; 14 h;
参考文献
Tashtoush, Hasan I.; Sustmann, Reiner
Chemische Berichte, 1993 , vol. 126, # 7 p. 1759 - 1762
90-14-2
1-碘萘
+
100200-86-0
→
反应条件
701974-97-2
反应条件
copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride T=20°C;
参考文献
Law, Charles C.W.; Lam, Jacky W.Y.; Dong, Yuping; Tong, Hui; Tang, Ben Zhong
Macromolecules, 2005 , vol. 38, # 3 p. 660 - 662
90-14-2
1-碘萘
+
766-97-2
4-甲苯基乙炔
→
反应条件
72735-70-7
反应条件
copper(l) iodide; N,N'-dibenzyl-BINAM; potassium carbonate in N,N-dimethyl-formamide T=140 - 145°C; Sonogashira coupling; 20 h; Inert atmosphere;
参考文献
Thakur; Jaseer; Naidu, Ajay B.; Sekar, Govindasamy
Tetrahedron Letters, 2009 , vol. 50, # 24 p. 2865 - 2869
624-31-7
4-碘甲苯
+
90-14-2
1-碘萘
+
1066-54-2
三甲基乙炔基硅
→
反应条件
72735-70-7
反应条件
1: 1-(iodo)-4-methylbenzene; trimethylsilylacetylene With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in toluene T=20°C; 18 h; Inert atmosphere; 2: monoiodonaphthalene With water; 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene T=20°C; 18 h; Inert atmosphere;
参考文献
Rakshit, Souvik; Patureau, Frederic W.; Glorius, Frank
Journal of the American Chemical Society, 2010 , vol. 132, # 28 p. 9585 - 9587
90-14-2
1-碘萘
→
反应条件
7495-56-9
反应条件
1: 1.) Mg / 1.) ether, reflux; 2.) benzene, reflux 2: 92 percent / LiAlH4 / diethyl ether / Heating View Scheme
参考文献
Cheung, Julie; Field, Leslie D.; Regaglia, Francesca; Sternhell, Sever
Australian Journal of Chemistry, 1995 , vol. 48, # 10 p. 1707 - 1726
90-14-2
1-碘萘
→
反应条件
7504-41-8
反应条件
1: 1.) Mg / 1.) ether, reflux; 2.) benzene, reflux 2: 92 percent / LiAlH4 / diethyl ether / Heating 3: 81 percent / pyridine 4: 75 percent / KI / H2O; dimethylformamide View Scheme
参考文献
Cheung, Julie; Field, Leslie D.; Regaglia, Francesca; Sternhell, Sever
Australian Journal of Chemistry, 1995 , vol. 48, # 10 p. 1707 - 1726
5765-65-1
+
90-14-2
1-碘萘
→
反应条件
7508-21-6
反应条件
bicyclo-[2.2.1]hept-2-ene; tris(4-methoxyphenyl)-phosphine; palladium diacetate; caesium carbonate; isopropyl alcohol in toluene T=100°C; 24 h; Inert atmosphereSealed tube;
参考文献
Dong, Zhe; Dong, Guangbin
Journal of the American Chemical Society, 2013 , vol. 135, # 49 p. 18350 - 18353
90-14-2
1-碘萘
+
108-98-5
→
反应条件
7570-98-1
反应条件
copper(l) iodide; potassium fluoride on basic alumina in N,N-dimethyl-formamide T=110°C; 8 h; Inert atmosphereCombinatorial reaction / High throughput screening (HTS);
参考文献
Feng, Yi-Si; Li, Yuan-Yuan; Tang, Lin; Wu, Wei; Xu, Hua-Jian
Tetrahedron Letters, 2010 , vol. 51, # 18 p. 2489 - 2492
90-14-2
1-碘萘
+
882-33-7
→
反应条件
7570-98-1
反应条件
copper(I) sulphide; iron; potassium carbonate; dimethyl sulfoxide T=110°C; 18 h; Inert atmosphere; chemoselective reaction;
参考文献
Wang, Huifeng; Jiang, Linlin; Chen, Tao; Li, Yarning
European Journal of Organic Chemistry, 2010 , # 12 p. 2324 - 2329
→
反应条件
7570-98-1
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=100°C; 4 h; Inert atmosphere;
参考文献
Lee, Jae-Young; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7413 - 7416
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