反应条件
1: 1.) hydrochloric acid, sodium nitrite, 2.) potassium iodide / 1.) water, 0 deg C, 45 min, 2.) water, overnight 2: 1.) tert-butyllithium / 1.) diethyl ether, pentane, -78 deg C, 1 h, 2.) diethyl ether, 30 min 3: 98 percent / hydrochloric acid, acetic acid / H2O / 0.33 h / Heating 4: 84 percent / acetic acid, sulfuric acid, iodic acid, iodine / H2O / 3 h / 80 °C View Scheme
参考文献
Wu, Ruilian; Schumm, Jeffry S.; Pearson, Darren L.; Tour, James M.
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 6906 - 6921
