triethylamine; phosphorus trichoride in toluene 18 h; Heating;
参考文献
Bedford, Robin B.; Hazelwood, Samantha L. Welch; Horton, Peter N.; Hursthouse, Michael B.
Journal of the Chemical Society. Dalton Transactions, 2003 , # 21 p. 4164 - 4174
N-ethyl-N,N-diisopropylamine; phosphorus trichoride in toluene T=-20 - 20°C; 14 h;
参考文献
Swennenhuis, Bert H. G.; Chen, Ruifang; Van Leeuwen, Piet W. N. M.; De Vries, Johannes G.; Kamer, Paul C. J.
Organic Letters, 2008 , vol. 10, # 5 p. 989 - 992
pinacol borane; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in tetrahydrofuran byproducts: H2; C6H5C6H4OH reacted with (C2H5)2SiH2 and Ir complex in C6H6, reacted withB compds., Ir complex and 4,4'-di-tert-butylpyridine in THF at 80.degre e.C, reacted with aq. KHF2 in THF; obtained contaminated;
参考文献
Boebel, Timothy A.; Hartwig, John F.
Journal of the American Chemical Society, 2008 , vol. 130, # 24 p. 7534 - 7535