3,4,5-三甲氧基肉桂酸合成路线 （共 18 条）
反应条件
potassium hydroxide 2 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 3 p. 810 - 821
反应条件
1: palladium-barium sulfate; xylene / Hydrogenation 2: pyridine; piperidine View Scheme
参考文献
Chemische Berichte, , vol. 63, p. 3029,3043
反应条件
alkaline permanganate T=60 - 65°C;
参考文献
Gadamer
Archiv der Pharmazie (Weinheim, Germany), 1897 , vol. 235, p. 110
Chemische Berichte, 1897 , vol. 30, p. 2331
反应条件
5 Pd(II)/C(eggshell); hydrogen in tetrahydrofuran T=20°C; P=1551.49 Torr; 3 h;
参考文献
Shan, Shao-Jun; Zhang, Hong; Wang, Xiao-Dan
Journal of Chemical Research, 2012 , vol. 36, # 1 p. 56 - 57
反应条件
hydroquinone in xylene
T=175°C;
参考文献
Perun,T.J. et al.
Journal of Organic Chemistry, 1963 , vol. 28, # 11 p. 2937 - 2943
参考文献
Levai; Duddeck
Pharmazie, 1983 , vol. 38, # 12 p. 827 - 828
反应条件
1: 92 percent / LiAlH4 / tetrahydrofuran / 2 h / 0 °C
2: Et3N / CH2Cl2 / 1 h
3: NaI / acetone / Heating
View Scheme
参考文献
Rosowsky, Andre; Papoulis, Andrew T.; Queener, Sherry F.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 6 p. 913 - 918
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C;
参考文献
Rosowsky, Andre; Chen, Han; Fu, Hongning; Queener, Sherry F.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 1 p. 59 - 67
