4,4'-二甲氧基二苯甲酮合成路线 (共 402 条)
反应条件
1: 2.) H2SO4 / 1.) ether, 2.) acetic acid, 70 - 80 deg C 2: O2, DCA / acetonitrile / 13 °C / Irradiation; also in the presence of LiClO4 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 22 p. 6049 - 6056
反应条件
iodine in neat (no solvent) T=85°C; 1.5 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 12 p. 1978 - 1999
反应条件
chromic acid; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 48, p. 3148
反应条件
in dichloromethane T=20°C; 240 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 4 p. 610 - 614
Zhurnal Organicheskoi Khimii, , vol. 19, # 4 p. 694 - 698
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-90°C; 0.25 h;
参考文献
Helvetica Chimica Acta, , vol. 84, # 11 p. 3319 - 3334
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-90°C; 0.25 h;
参考文献
Helvetica Chimica Acta, , vol. 84, # 11 p. 3319 - 3334
反应条件
zeolite; oxygen in hexane UV-irradiation;
参考文献
Organic Letters, , vol. 5, # 26 p. 4979 - 4982
反应条件
tetrakis-(ethylene)-μ,μ'-dichlorodirhodium(I); n-butyl-triphenylphosphonium bromide in toluene T=165°C; 24 h; Heating;
参考文献
Rao, Honghua; Yang, Luo; Shuai, Qi; Li, Chao-Jun
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1701 - 1706
反应条件
pyridine; iodine in tetrahydrofuran T=20°C;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 25 p. 4943 - 4953
反应条件
Nitrous oxide T=280°C; P=367754 Torr;
参考文献
Journal of the Chemical Society, , p. 2999,3006