4,4'-二甲氧基二苯甲酮合成路线 (共 402 条)
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); di-tert-butyl peroxide; 1,2-bis-(diphenylphosphino)ethane in benzene T=160°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Yang, Luo; Zeng, Tieqiang; Shuai, Qi; Guo, Xiangyu; Li, Chao-Jun
Chemical Communications, 2011 , vol. 47, # 7 p. 2161 - 2163
反应条件
sodium methylate; tris(dibenzylideneacetone)dipalladium (0) in chloroform T=20°C; P=760 Torr; 3 h;
参考文献
Kang; Ryu; Choi
Synthetic Communications, 2001 , vol. 31, # 7 p. 1035 - 1039
反应条件
RhH(CO)(triphenylphosphine)3 in methanol T=80°C; P=15001.2 Torr; 18 h;
参考文献
Chemical Communications, , # 13 p. 1520 - 1521
反应条件
tetra-(n-butyl)ammonium iodide; (Ph3P)2Pd(Ph)(I) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=25°C;
参考文献
Bumagin, N. A.; Kalinovskii, I. O.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 211
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 221
反应条件
hexaethyl distannane; triethyl phosphite; bis(η3-allyl-μ-chloropalladium(II)) in toluene T=111°C; 2 h;
参考文献
Journal of Organometallic Chemistry, , vol. 282, p. 421 - 426
反应条件
mercury(II) fluoride; oxygen in acetonitrile T=25°C; 24 h; Irradiation;
参考文献
Farhadi, Saeid; Zaringhadam, Parisa; Sahamieh, Reza Zarei
Tetrahedron Letters, 2006 , vol. 47, # 12 p. 1965 - 1968
反应条件
tris-(o-tolyl)phosphine; palladium diacetate in toluene T=20°C; 24 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 2 p. 331 - 340
反应条件
1: carbon monoxide With 1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran T=20°C; P=760.051 Torr; 0.166667 h; 2: 4-methoxyphenylzinc iodide With ethylene dibromide in tetrahydrofuran T=60°C; 3 h;
参考文献
Kobayashi, Kana; Nishimura, Yugo; Gao, Fuxing; Gotoh, Kazuma; Nishihara, Yasushi; Takagi, Kentaro
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1949 - 1952
反应条件
Ni(Br)2(dppe); zinc in tetrahydrofuran T=110°C; 24 h;
参考文献
Huang, Yi-Chun; Majumdar, Kanak Kanti; Cheng, Chien-Hong
Journal of Organic Chemistry, 2002 , vol. 67, # 5 p. 1682 - 1684
反应条件
bromine in tetrachloromethane T=30 - 40°C; 0.0833333 h;
参考文献
Caputo, Romualdo; Ferreri, Carla; Palumbo, Giovanni; Capozzi, Giuseppe
Tetrahedron, 1986 , vol. 42, # 8 p. 2369 - 2376