4,4'-二甲氧基二苯甲酮合成路线 (共 402 条)
参考文献
van Alphen
Recueil des Travaux Chimiques des Pays-Bas, 1930 , vol. 49, p. 153,159
Full Text Show Details
Pohlmann
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 737,740
反应条件
1: in xylene T=20°C; 0.25 h; 2: With diethylaluminium chloride in toluene; xylene 3: With water in tetrahydrofuran; toluene; xylene Heating;
参考文献
Kwan, Man Lung; Battiste, Merle A
Tetrahedron Letters, 2002 , vol. 43, # 48 p. 8765 - 8768
反应条件
1: With triethylamine T=20°C; Peterson reaction; 1 h; 2: With diethylaluminium chloride Peterson olefination; 12 h; Heating;
参考文献
Kwan, Man Lung; Battiste, Merle A.; Macala, Megan K.; Aybar, Sylvia C.; James, Nicholas C.; Haoui, Joseph J.
Synthetic Communications, 2004 , vol. 34, # 11 p. 1943 - 1950
反应条件
2: CH3COCl / benzene View Scheme
参考文献
Blumenstock, H.; Dickert, F.; Fackler, H.; Hammerschmidt, A.
Zeitschrift fuer Physikalische Chemie (Muenchen, Germany), 1983 , vol. 135, p. 157 - 170
反应条件
1: SOCl2 / Erwaermen auf dem Dampfbad 2: diethyl ether View Scheme
参考文献
Schoenberg; Urban
Chemische Berichte, 1934 , vol. 67, p. 1999,2000
反应条件
potassium hydroxide; oxygen in ethylene glycol dimethyl ether T=70 - 80°C; 10 h;
参考文献
Artamkina, G. A.; Grinfel'd, A. A.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 2 p. 345 - 352
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 2 p. 383 - 391
参考文献
Swan
Journal of the Chemical Society, 1948 , p. 1408,1411
反应条件
hydrazine hydrate in toluene Condensation; 0.166667 h; microwave irradiation;
参考文献
Gadhwal, Sunil; Baruah, Mukulesh; Sandhu, Jagir S.
Synlett, 1999 , # 10 p. 1573 - 1574
反应条件
1: NH2OH*HCl / pyridine / Heating 2: (i) EtONa, EtOH, (ii) /BRN= 1209223/ View Scheme
参考文献
Smith,P.A.S.; Robertson,J.E.
Journal of the American Chemical Society, 1962 , vol. 84, p. 1197 - 1204
反应条件
iodine in neat (no solvent) T=85°C; 8 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 12 p. 1978 - 1999