4,4'-二甲氧基二苯甲酮合成路线 （共 402 条）
参考文献
van Alphen
Recueil des Travaux Chimiques des Pays-Bas, 1930 , vol. 49, p. 153,159
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Pohlmann
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 737,740
参考文献
van Alphen
Recueil des Travaux Chimiques des Pays-Bas, 1930 , vol. 49, p. 153,159
反应条件
1: (9H-fluoren-9-yl)trimethylsilane With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 0°C;
2: 1,1-di(p-methoxyphenyl)-ketone in tetrahydrofuran; hexane
T=20°C; Peterson olefination; 12 h; Further stages.;
参考文献
Mills, Nancy S.; Benish, Michele A.; Ybarra, Christie
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2003 - 2012
反应条件
n-butyllithium in tetrahydrofuran
T=-78°C;
参考文献
Gu, Xinggui; Yao, Jingjing; Zhang, Guanxin; Yan, Yongli; Zhang, Chuang; Peng, Qian; Liao, Qing; Wu, Yishi; Xu, Zhenzhen; Zhao, Yongsheng; Fu, Hongbing; Zhang, Deqing
Advanced Functional Materials, 2012 , vol. 22, # 23 p. 4862 - 4872
反应条件
1: n-butyllithium / hexane; tetrahydrofuran / 1.) 30 min, -100 deg C; 2.) -100 deg C, 1 h
2: H2SO4 / benzene / Heating
View Scheme
参考文献
Franco, M. Luisa T. M. B.; Herold, Bernardo J.; Evans, Jeffrey C.; Rowlands, Christopher C.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 443 - 450
参考文献
Taylor, Edward C.; Davies, Huw M. L.
Tetrahedron Letters, 1983 , vol. 24, # 49 p. 5453 - 5456
反应条件
1: 65 percent
2: 84 percent / p-(n-dodecyl)benzenesulfonyl azide
View Scheme
参考文献
Taylor, Edward C.; Davies, Huw M. L.
Tetrahedron Letters, 1983 , vol. 24, # 49 p. 5453 - 5456
反应条件
2: CH3COCl / benzene
3: acetonitrile
View Scheme
参考文献
Blumenstock, H.; Dickert, F.; Fackler, H.; Hammerschmidt, A.
Zeitschrift fuer Physikalische Chemie (Muenchen, Germany), 1983 , vol. 135, p. 157 - 170
反应条件
2: with sulfuric acid impregnated pumice stone / 300 °C
3: aqueous ether; iodine; HgO / und Behandeln des Reaktionsprodukts mit AgNO3-Loesung
View Scheme
参考文献
Weill
Bulletin de la Societe Chimique de France, 1931 , vol. <4> 49, p. 1811,1822
反应条件
1: diethyl ether / 1 h
2: p-toluenesulfonic acid / benzene / Heating
View Scheme
参考文献
Kao, Hsien-Ming; Grey, Clare P.; Pitchumani, Kasi; Lakshminarasimhan; Ramamurthy
Journal of Physical Chemistry A, 1998 , vol. 102, # 28 p. 5627 - 5638
