4,4'-二甲氧基二苯甲酮合成路线 （共 402 条）
参考文献
Blicke; Weinkauff
Journal of the American Chemical Society, 1932 , vol. 54, p. 1446,1451
反应条件
1: ethanol; sodium-amalgam
2: benzene; HCl
3: benzene; fine-dispersed silver / unter Kohlendioxyd
View Scheme
参考文献
Nauta; Mulder
Recueil des Travaux Chimiques des Pays-Bas, 1939 , vol. 58, p. 1062,1065
反应条件
(i) LiNH2, liq. NH3, (ii) /BRN= 1878026/; Multistep reaction;
参考文献
Kaiser,E.M. et al.
Journal of Organometallic Chemistry, 1973 , vol. 59, p. 53 - 64
反应条件
1: C9H16N2*C3H2F6O2 With potassium tert-butylate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide
T=-30°C; 0.5 h;
2: 1,1-di(p-methoxyphenyl)-ketone in N,N-dimethyl-formamide
T=-30°C; 1.5 h;
参考文献
Riofski, Mark V.; Hart, Allison D.; Colby, David A.
Organic Letters, 2013 , vol. 15, # 1 p. 208 - 211
反应条件
1: 2,2,2-trifluoroethane-1,1-diol With potassium tert-butylate in N,N-dimethyl-formamide
T=-50°C; 0.583333 h;
2: 1,1-di(p-methoxyphenyl)-ketone in N,N-dimethyl-formamide
T=-50°C; 1 h;
参考文献
Surya Prakash; Zhang, Zhe; Wang, Fang; Munoz, Socrates; Olah, George A.
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3300 - 3305
反应条件
1: tetramethylammonium fluoride / tetrahydrofuran / a) O deg C, 30 min, b) 25 deg C, 16 h
2: 10percent aq.HF / tetrahydrofuran / 5 h
View Scheme
参考文献
Ahvazi, Behzad C.; Crestini, Claudia; Argyropoulos, Dimitris S.
Journal of Agricultural and Food Chemistry, 1999 , vol. 47, # 1 p. 190 - 201
反应条件
diethyl ether
spaeter in Benzol;
参考文献
Gomberg; Snow
Journal of the American Chemical Society, 1925 , vol. 47, p. 209
反应条件
1: 77.8 percent / Br2 / acetic acid / 1 h
2: 85 percent / pyridine*HCl / 0.33 h / 210 °C
View Scheme
参考文献
Lesiak, T.; Nowakowski, J.
Journal fuer Praktische Chemie (Leipzig), 1981 , vol. 323, # 4 p. 684 - 690
反应条件
ethanol; hydroxylamine
参考文献
Harada; Ohno; Kobayashi; Mukaiyama
Synthesis, 1991 , # 12 p. 1216 - 1220
反应条件
potassium tert-butylate; tert-butyl alcohol
Erwaermen des Reaktionsprodukts mit wss.-aethanol. KOH;
参考文献
Johnson; Miller
Journal of the American Chemical Society, 1950 , vol. 72, p. 511
