4,4'-二甲氧基二苯甲酮合成路线 (共 402 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethylene glycol dimethyl ether P=760 Torr; 1 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Lim, Kwon-Ho; Ho, Pil-Su; Yoon, Seok-Keun; Son, Hoe-Joo
Synthetic Communications, 1998 , vol. 28, # 8 p. 1481 - 1489
反应条件
copper dichloride; palladium dichloride in acetonitrile T=25°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 74, # 7 p. 1343 - 1348
反应条件
air; 2,3-dimethyl-naphthalene in acetonitrile 0.00277778 h; microwave irradiation;
参考文献
Enquist, Per-Anders; Nilsson, Peter; Larhed, Mats
Organic Letters, 2003 , vol. 5, # 25 p. 4875 - 4878
反应条件
1: bromodifluoromethyl phenyl sulphide With AlCl3, aluminium chloride in dichloromethane T=20°C; Friedel Crafts type alkylation; 0.25 h; Inert atmosphere; 2: methoxybenzene in dichloromethane T=20°C; Friedel Crafts type alkylation; 16 h; Inert atmosphere;
参考文献
Kuhakarn, Chutima; Surapanich, Nakin; Kamtonwong, Siriporn; Pohmakotr, Manat; Reutrakul, Vichai
European Journal of Organic Chemistry, 2011 , # 29 p. 5911 - 5918
反应条件
1: p-MeOC6H4ZnCl With tetrabutylammomium bromide; palladium diacetate in tetrahydrofuran T=20°C; Negishi coupling reaction; 0.0833333 h; Inert atmosphere; 2: 4-methoxy-benzoyl chloride in tetrahydrofuran T=20°C; Negishi coupling reaction; 1 h; Inert atmosphere;
参考文献
Yu, Lei; Ren, Lingfeng; Chen, Tian; Yi, Rong; Wu, Yulan; Guo, Rong
Organic Preparations and Procedures International, 2012 , vol. 44, # 2 p. 169 - 174
反应条件
potassium phosphate; oxygen; copper diacetate; p-toluidine; sodium sulfate in dimethyl sulfoxide T=140°C; 6 h; Sealed tube;
参考文献
Maji, Arun; Rana, Sujoy; Akanksha; Maiti, Debabrata
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2428 - 2432
Angew. Chem., 2014 , vol. 126, # 9 p. 2460 - 2464,5
反应条件
dichloro-acetic acid; oxygen in acetonitrile 0.916667 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 34, # 16 p. 2641 - 2644
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-90°C; 0.00416667 h;
参考文献
Helvetica Chimica Acta, , vol. 83, # 12 p. 3163 - 3178
反应条件
tin(IV) chloride in dichloromethane T=-78°C; 0.25 h;
参考文献
Helvetica Chimica Acta, , vol. 84, # 11 p. 3319 - 3334
反应条件
silica gel in dichloromethane T=20°C; 1.66667 h;
参考文献
Helvetica Chimica Acta, , vol. 86, # 8 p. 2833 - 2847