4,4'-二甲氧基二苯甲酮合成路线 (共 402 条)
反应条件
silica gel in dichloromethane T=20°C; 8 h;
参考文献
Helvetica Chimica Acta, , vol. 86, # 8 p. 2833 - 2847
反应条件
1: 86 percent / TiCl4 / CH2Cl2 / 2.5 h / 20 °C 2: 98 percent / iron(III) acetylacetonate / tetrahydrofuran / 0 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 22 p. 2968 - 2970
反应条件
potassium phosphate; oxygen; copper diacetate; p-toluidine; sodium sulfate in dimethyl sulfoxide T=140°C; 2 h; Sealed tube;
参考文献
Maji, Arun; Rana, Sujoy; Akanksha; Maiti, Debabrata
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2428 - 2432
Angew. Chem., 2014 , vol. 126, # 9 p. 2460 - 2464,5
反应条件
oxygen; Manganese (II) acetate in acetic acid T=23°C; 12 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 5 p. 1371 - 1378
反应条件
sodium hydroxide; tetrabutylammomium bromide; dicobalt octacarbonyl; pentacarbonyliron(0) in water; benzene T=65°C; 48 h; Further byproducts given;
参考文献
Journal of Organometallic Chemistry, , vol. 384, p. 193 - 197
反应条件
methyltrioxorhenium (VII) in benzene 48 h; Ambient temperature;
参考文献
Zhu, Zuolin; Espenson, James H.
Journal of Organic Chemistry, 1996 , vol. 61, # 1 p. 324 - 328
反应条件
copper dichloride; palladium dichloride in acetic acid T=25°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 74, # 7 p. 1343 - 1348
反应条件
1: 67 percent Spectr. / tetra-n-butylammonium nitrite / acetonitrile / 3 h / 20 °C 2: 53 percent / 48 h / 0 °C 3: 89 percent / tetra-n-butylammonium nitrite / acetonitrile; benzene / 3 h / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 29 p. 4623 - 4626
反应条件
1: 86 percent Chromat. / methyl vinyl ketone / Ru3(CO)12 / acetone; dioxane / 1 h / Heating 2: aq. HCl / tetrahydrofuran / 12 h View Scheme
参考文献
Chemical Communications, , # 9 p. 1185 - 1187
反应条件
1: 86 percent Chromat. / methyl vinyl ketone / Ru3(CO)12 / acetone; dioxane / 1 h / Heating 2: aq. HCl / tetrahydrofuran / 12 h View Scheme
参考文献
Chemical Communications, , # 9 p. 1185 - 1187