4,4'-二甲氧基二苯甲酮合成路线 (共 402 条)
反应条件
1: methanol With N-benzyl-trimethylammonium hydroxide 0.166667 h; Neat (no solvent); 2: 1,1-di(p-fluorophenyl)-ketone T=20°C; 0.166667 h; Neat (no solvent);
参考文献
Meshram; Goud, P. Ramesh; Reddy, B. Chennakesava; Kumar, D. Aravind
Synthetic Communications, 2010 , vol. 40, # 14 p. 2122 - 2129
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I); di-tert-butyl peroxide; triphenylphosphine in benzene T=150°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Chemical Communications, , vol. 47, # 7 p. 2161 - 2163
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; copper diacetate in 1,4-dioxane T=70°C; 2 h; Inert atmosphere;
参考文献
Australian Journal of Chemistry, , vol. 65, # 12 p. 1687 - 1690
反应条件
Mn(III) acetylacetonate in acetic acid 0.0166667 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 7 p. 1922 - 1927
反应条件
tetrakis(triphenylphosphine) palladium(0) in methanol T=25°C; P=760 Torr; 20 h;
参考文献
Journal of Organometallic Chemistry, , vol. 344, p. C5 - C7
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-90°C; 0.25 h;
参考文献
Helvetica Chimica Acta, , vol. 84, # 11 p. 3319 - 3334
反应条件
iron silicate T=25°C; Friedel-Crafts acylation;
参考文献
Borate, Hanumant B.; Gaikwad, Abaji G.; Maujan, Suleman R.; Sawargave, Sangmeshwer P.; Kalal, Kamalakar M.
Tetrahedron Letters, 2007 , vol. 48, # 28 p. 4869 - 4872
反应条件
1: 53 percent / 48 h / 0 °C 2: 89 percent / tetra-n-butylammonium nitrite / acetonitrile; benzene / 3 h / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 29 p. 4623 - 4626
反应条件
1: 1) H2SO4 / 2) r.t., 4-5h 2: Ac2O 3: 35 percent / AlCl3 / (anisole) / nitrobenzene / 6 h / 55 - 60 °C / anisole not necessary for the reaction because it does not react with VII in the expected manner 4: alkal.KMnO4 View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 7 p. 572 - 574
反应条件
caesium carbonate; palladium dichloride in N,N-dimethyl acetamide T=100°C; 20 h;
参考文献
Organic Letters, , vol. 13, # 14 p. 3648 - 3651