4,4'-二氯二苯甲酮合成路线 （共 275 条）
反应条件
1: 1-chloro-4-bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: 4-chlorobenzaldehyde in tetrahydrofuran; hexane T=-78 - 20°C; 1 h; 3: With iodine; potassium carbonate in tert-butyl alcohol 3 h; Reflux;
参考文献
Ushijima, Sousuke; Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 5 p. 1436 - 1442
反应条件
chromium(VI) oxide in neat (no solvent) T=20°C; 0.00833333 h;
参考文献
He, Ai; Zhang, Jie; Zheng, Wenjin; Huang, Chen; Zhang, Changhe; Huang, Lihong; Lou, Ji-Dong
Research on Chemical Intermediates, 2013 , vol. 39, # 3 p. 1015 - 1020
参考文献
Mil'to, V. I.; Mironov, G. S.; Kopeikin, V. V.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 11.2 p. 2139 - 2141
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 11 p. 2372 - 2374
反应条件
hexaethyl distannane; triethyl phosphite; bis(η3-allyl-μ-chloropalladium(II)) in toluene T=111°C; 2 h;
参考文献
Journal of Organometallic Chemistry, , vol. 282, p. 421 - 426
反应条件
sodium hypochlorite in acetonitrile T=20°C; 4 h;
参考文献
Khurana; Sharma; Gogia; Kandpal
Organic Preparations and Procedures International, 2007 , vol. 39, # 2 p. 185 - 189
反应条件
rhenic(VII) acid in toluene 24 h; Reflux;
参考文献
Tetrahedron Letters, , vol. 53, # 46 p. 6205 - 6208,4
反应条件
potassium carbonate in methoxybenzene T=80°C; carbonylative Suzuki-Miyaura cross-coupling; P=760.051 Torr; 6 h;
参考文献
Cai, Mingzhong; Peng, Jian; Hao, Wenyan; Ding, Guodong
Green Chemistry, 2011 , vol. 13, # 1 p. 190 - 196
反应条件
copper dichloride; palladium dichloride in acetonitrile T=25°C; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 74, # 7 p. 1343 - 1348
反应条件
palladium diacetate; indium in N,N-dimethyl-formamide T=20°C; P=760 Torr; 1 h;
参考文献
Zhou, Tao; Chen, Zhen-Chu
Synthetic Communications, 2002 , vol. 32, # 22 p. 3431 - 3435
反应条件
mercury(II) fluoride; oxygen in acetonitrile T=25°C; 24 h; Irradiation;
参考文献
Farhadi, Saeid; Zaringhadam, Parisa; Sahamieh, Reza Zarei
Tetrahedron Letters, 2006 , vol. 47, # 12 p. 1965 - 1968
