(2-碘苯甲酰基)乙酸乙酯合成路线 (共 3 条)
反应条件
hydrogenchloride; n-butyllithium; sodium hydrogencarbonate in tetrahydrofuran; hexane; nitrogen; ethyl acetate
反应条件
ammonium hydroxide; sodium hydroxide; water; ammonium chloride T=50°C; 3 h;
参考文献
Sicker, Dieter; Mann, Gerhard
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 4 p. 839 - 850
反应条件
1: 1) Mg, EtOH / 1) CCl4, toluene; 2) -5 to 0 deg C 2: 65 percent / NaOH, H2O, NH4Cl, conc. NH4OH / 3 h / 50 °C View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 53, # 4 p. 839 - 850