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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
90047-72-6
合成路线
（共 7 条）
90047-72-6
→
反应条件
5487-33-2
(3-苄氧基-4-甲氧基-苯基)乙酸
反应条件
sodium tetrahydroborate; diphenyl diselenide; sodium hydroxide in ethanol T=40°C; 18 h;
参考文献
Schrittwieser, Joerg H.; Resch, Verena; Wallner, Silvia; Lienhart, Wolf-Dieter; Sattler, Johann H.; Resch, Jasmin; MacHeroux, Peter; Kroutil, Wolfgang
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6703 - 6714
90047-72-6
→
反应条件
485-19-8
牛心果碱
+
605-34-5
分离木瓣树胺
反应条件
1.1: sodium tetrahydroborate; diphenyl diselenide; sodium hydroxide / ethanol / 18 h / 40 °C 2.1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 1 h / 20 °C / Inert atmosphere 3.1: sodium hydroxide / chloroform / 0 - 20 °C 4.1: trichlorophosphate / acetonitrile / 3 h / Reflux; Inert atmosphere 4.2: 20 °C / Inert atmosphere; Cooling with ice 5.1: palladium 10 on activated carbon; hydrogen; acetic acid / methanol / 16 h 6.1: berberine bridge enzyme; tris(hydroxymethyl)methylamine hydrochloride; magnesium chloride / toluene / 24 h / 40 °C / pH 9 / Darkness; Enzymatic reaction View Scheme
参考文献
Schrittwieser, Joerg H.; Resch, Verena; Wallner, Silvia; Lienhart, Wolf-Dieter; Sattler, Johann H.; Resch, Jasmin; MacHeroux, Peter; Kroutil, Wolfgang
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6703 - 6714
67-66-3
氯仿
+
6346-05-0
3-苄氧基-4-甲氧基苯甲醛
→
反应条件
90047-72-6
反应条件
potassium hydroxide in methanol; N,N-dimethyl-formamide T=-10°C; 2.5 h; Inert atmosphere;
参考文献
Schrittwieser, Joerg H.; Resch, Verena; Wallner, Silvia; Lienhart, Wolf-Dieter; Sattler, Johann H.; Resch, Jasmin; MacHeroux, Peter; Kroutil, Wolfgang
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6703 - 6714
621-59-0
3-羟基-4-甲氧基苯甲醛
→
反应条件
90047-72-6
反应条件
1: potassium carbonate / ethanol / 20 h / 20 °C / Inert atmosphere 2: potassium hydroxide / methanol; N,N-dimethyl-formamide / 2.5 h / -10 °C / Inert atmosphere View Scheme
参考文献
Schrittwieser, Joerg H.; Resch, Verena; Wallner, Silvia; Lienhart, Wolf-Dieter; Sattler, Johann H.; Resch, Jasmin; MacHeroux, Peter; Kroutil, Wolfgang
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6703 - 6714
100-39-0
溴化苄
→
反应条件
90047-72-6
反应条件
1: potassium carbonate / ethanol / 20 h / 20 °C / Inert atmosphere 2: potassium hydroxide / methanol; N,N-dimethyl-formamide / 2.5 h / -10 °C / Inert atmosphere View Scheme
参考文献
Schrittwieser, Joerg H.; Resch, Verena; Wallner, Silvia; Lienhart, Wolf-Dieter; Sattler, Johann H.; Resch, Jasmin; MacHeroux, Peter; Kroutil, Wolfgang
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6703 - 6714
90047-72-6
→
反应条件
54313-33-6
2-(3-(苄氧基)-4-甲氧基苯基)乙酰氯
反应条件
1: sodium tetrahydroborate; diphenyl diselenide; sodium hydroxide / ethanol / 18 h / 40 °C 2: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 1 h / 20 °C / Inert atmosphere View Scheme
参考文献
Resch, Verena; Lechner, Horst; Schrittwieser, Joerg H.; Wallner, Silvia; Gruber, Karl; MacHeroux, Peter; Kroutil, Wolfgang
Chemistry - A European Journal, 2012 , vol. 18, # 41 p. 13173 - 13179
90047-72-6
→
反应条件
485-19-8
牛心果碱
+
605-34-5
分离木瓣树胺
反应条件
1.1: sodium tetrahydroborate; diphenyl diselenide; sodium hydroxide / ethanol / 18 h / 40 °C 2.1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 1 h / 20 °C / Inert atmosphere 3.1: sodium hydroxide / chloroform / 0 - 20 °C 4.1: trichlorophosphate / acetonitrile / 3 h / Reflux; Inert atmosphere 4.2: 20 °C / Inert atmosphere; Cooling with ice 5.1: palladium 10 on activated carbon; hydrogen; acetic acid / methanol / 16 h 6.1: berberine bridge enzyme; tris(hydroxymethyl)methylamine hydrochloride; magnesium chloride / toluene / 24 h / 40 °C / pH 9 / Darkness; Enzymatic reaction View Scheme
参考文献
Schrittwieser, Joerg H.; Resch, Verena; Wallner, Silvia; Lienhart, Wolf-Dieter; Sattler, Johann H.; Resch, Jasmin; MacHeroux, Peter; Kroutil, Wolfgang
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6703 - 6714
