N-甲基-3-溴-5-硝基苯甲酰胺合成路线 （共 3 条）
反应条件
1: 5-Bromo-3-nitrobenzoic acid With oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane 2 h; 2: methylamine in tetrahydrofuran T=0°C;
参考文献
Batt, Douglas G.
Patent: US2004/67935 A1, 2004 ;
Location in patent: Page/Page column 33 ;
US 20040067935 A1
反应条件
1: 5-Bromo-3-nitrobenzoic acid With oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane T=20°C; 5 h; 2: methylamine in tetrahydrofuran T=0 - 20°C; 14 h;
参考文献
WO2007/48771 A1, ;
Page/Page column 23-24; 57 ;
WO 2007/048771 A1
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 18, # 2 p. 576 - 585
