4,4’-(1,8-辛二氧基)二苯胺合成路线 (共 5 条)
反应条件
sodium sulfide in ethanol; water
Reduction; Heating;
参考文献
Imrie, Corrie T.; Stewart, David; Rerny, Catherine; Christie, David W.; Hamley; Harding
Journal of Materials Chemistry, 1999 , vol. 9, # 10 p. 2321 - 2325
反应条件
1: 71 percent / K2CO3 / dimethylformamide / Heating
2: 35 percent / Na2S*9H2O / ethanol; H2O / Heating
View Scheme
参考文献
Imrie, Corrie T.; Stewart, David; Rerny, Catherine; Christie, David W.; Hamley; Harding
Journal of Materials Chemistry, 1999 , vol. 9, # 10 p. 2321 - 2325
反应条件
1: anhydous K2CO3 / dimethylformamide / 4 h / Heating
2: HCl / ethanol
3: NaHCO3 / H2O / 1 h
View Scheme
参考文献
Griffin; Britt; Hung; Steele
Molecular crystals and liquid crystals, 1983 , vol. 105, # 1-4 p. 305 - 314
反应条件
1: HCl / ethanol
2: NaHCO3 / H2O / 1 h
View Scheme
参考文献
Griffin; Britt; Hung; Steele
Molecular crystals and liquid crystals, 1983 , vol. 105, # 1-4 p. 305 - 314
反应条件
(i) aq. KOH, EtOH, (ii) aq. NaOH, EtOH; Multistep reaction;
参考文献
Rault,J. et al.
Bulletin de la Societe Chimique de France, 1975 , p. 1175 - 1178