2-苯甲酰氨基-3-[4-(双(2-羟基乙基)氨基)苯基]丙-2-烯酸甲酯合成路线 (共 4 条)
反应条件
in methanol
0.333333 h; Heating;
参考文献
Sen, A.K.; Mukhopadhyay, Sankardeb
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 939 - 941
反应条件
1: 56 percent / pyridine / 24 h / Ambient temperature
2: 52 percent / methanol / 0.33 h / Heating
View Scheme
参考文献
Sen, A.K.; Mukhopadhyay, Sankardeb
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 939 - 941
反应条件
1: 56 percent / pyridine / 24 h / Ambient temperature
2: 52 percent / methanol / 0.33 h / Heating
View Scheme
参考文献
Sen, A.K.; Mukhopadhyay, Sankardeb
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 939 - 941
反应条件
1: 70 percent / H2 / Raney Ni / methanol / 40 °C / 3361.5 Torr
2: 1.) POCl3, 2.) conc. HCl / 1.) benzene, reflux, 15 min, 2.) reflux, 4 h
View Scheme
参考文献
Sen, A.K.; Mukhopadhyay, Sankardeb
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 939 - 941