反应条件
1: 89 percent / m-chloroperbenzoic acid / CH2Cl2 / 1 h / 0 °C
2: 1.) BF3*OEt2, 2.) TiCl4 / 1.) CH2Cl2, -78 deg C, 5 min, 2.) -78 deg C, 1 h; -78 deg C - 0 deg C, 2 h
View Scheme
参考文献
Fleming, Ian; Newton, Trevor W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 119 - 124