氢氧化4-(2-(6-(二丁基氨基)-2-萘基)乙烯基)-1-(3-硫代丙基)吡啶正离子内盐合成路线 （共 4 条）
反应条件
in dichloromethane
T=20°C; 24 h;
参考文献
Hassner, A.; Birnbaum, D.; Loew, L. M.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2546 - 2551
反应条件
1: 77 percent / tri-o-tolylphosphine / palladium diacetate / triethylamine / 72 h / 110 °C
2: 56 percent / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Hassner, A.; Birnbaum, D.; Loew, L. M.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2546 - 2551
反应条件
1: 70 percent / potassium carbonate / dimethylformamide / 20 h / 130 °C
2: 77 percent / tri-o-tolylphosphine / palladium diacetate / triethylamine / 72 h / 110 °C
3: 56 percent / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Hassner, A.; Birnbaum, D.; Loew, L. M.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2546 - 2551
反应条件
1: 77 percent / tri-o-tolylphosphine / palladium diacetate / triethylamine / 72 h / 110 °C
2: 56 percent / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Hassner, A.; Birnbaum, D.; Loew, L. M.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2546 - 2551
