4-(二丁基氨基)苯甲醛合成路线 （共 13 条）
反应条件
trichlorophosphate T=95°C; 7.25 h; Cooling with iceInert atmosphere;
参考文献
Sarma, Monima; Chatterjee, Tanmay; Ghanta, Susanta; Das, Samar K.
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 432 - 444
反应条件
1: With potassium carbonate in dimethyl sulfoxide 0.25 h; sonication; 2: in dimethyl sulfoxide T=100°C; 48 h;
参考文献
Van Den Berg, Otto; Sengers, Wilco G.F.; Jager, Wolter F.; Picken, Stephen J.; Wuebbenhorst, Michael
Macromolecules, 2004 , vol. 37, # 7 p. 2460 - 2470
参考文献
Journal of the Chemical Society, , p. 1159,1162
反应条件
hydrogenchloride anschliessendes Erwaermen mit 4-Nitroso-N.N-dimethyl-anilin-hydrochlorid und Behandeln des nach der Hydrolyse mit wss. Natronlauge erhaltenen Reaktionsprodukts mit wss. Formaldehyd und Essigsaeure;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1890,1891
反应条件
1: 82 percent / K2CO3 / dimethylformamide / 10 h / 120 °C 2: 68 percent / phosphoryl trichloride / 4 h / 60 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 41 p. 10290 - 10299
反应条件
1: 30 h / Heating 2: AcOH / 2 h / 100 °C View Scheme
参考文献
Biochemical Pharmacology, , vol. 50, # 3 p. 399 - 406
参考文献
Journal of Organic Chemistry, , vol. 49, # 14 p. 2546 - 2551
反应条件
1: [3-(1,3-dioxolan-2-yl)allyl]phosphonic acid diethyl ester With potassium tert-butylate in tetrahydrofuran T=-78°C; Horner-Wadsworth-Emmons reaction; 1.5 h; 2: 4-[N,N-bis(n-butyl)amino]benzaldehyde in tetrahydrofuran T=0°C; 12 h;
参考文献
Lemercier, Gilles; Martineau, Cecile; Mulatier, Jean-Christophe; Wang, Irene; Stephan, Olivier; Baldeck, Patrice; Andraud, Chantal
New Journal of Chemistry, 2006 , vol. 30, # 11 p. 1606 - 1613
反应条件
1: NaH; 18-crown-6 / tetrahydrofuran / 20 h / 20 °C 2: HCl; H2O / tetrahydrofuran / 1 h / 20 °C 3: NaH; 18-crown-6 / tetrahydrofuran / 20 h / 20 °C 4: HCl; H2O / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Blanchard-Desce; Alain; Bedworth; Marder; Fort; Runser; Barzoukas; Lebus; Wortmann
Chemistry - A European Journal, 1997 , vol. 3, # 7 p. 1091 - 1104
反应条件
potassium hydroxide in ethanol Heating;
参考文献
Bahner,C.T. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 390 - 392
