4-(二丁基氨基)苯甲醛合成路线 （共 13 条）
反应条件
1: triphenyl-methyl-phosphonium iodide With n-butyllithium in tetrahydrofuran; hexane T=-80 - 20°C; 2 h; 2: 4-[N,N-bis(n-butyl)amino]benzaldehyde in tetrahydrofuran; hexane T=20°C; Wittig reaction;
参考文献
Wei, Peng; Bi, Xiangdong; Wu, Zhe; Xu, Zhi
Organic Letters, 2005 , vol. 7, # 15 p. 3199 - 3202
反应条件
1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane 2: 4-[N,N-bis(n-butyl)amino]benzaldehyde in tetrahydrofuran; hexane T=20°C; Wittig reaction; 24 h; Further stages.;
参考文献
Patrick, Michael J.; Ernst, Lauren A.; Waggoner, Alan S.; Thai, Dung; Tai, Dean; Salama, Guy
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 20 p. 3347 - 3353
反应条件
pyrrolidine in ethanol
Heating;
参考文献
Hassner, A.; Birnbaum, D.; Loew, L. M.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2546 - 2551
