N-(2-溴-5-硝基苯基)乙酰胺合成路线 （共 18 条）
反应条件
1: potassium carbonate / N,N-dimethyl-formamide 2: sodium formate; sodium acetate / palladium diacetate / N,N-dimethyl-formamide 3: Pd-C / methanol View Scheme
反应条件
sodium hydrogencarbonate in ethanol; water
参考文献
Chandramohan,M.R. et al.
Indian Journal of Chemistry, 1969 , vol. 7, p. 1006 - 1009
反应条件
1: sulfur; ethanol; Na2S 2: tin; aqueous HCl View Scheme
参考文献
Fries; Wolter
Justus Liebigs Annalen der Chemie, 1937 , vol. 527, p. 60,69
反应条件
sodium sulfide; ethanol; sulfur
参考文献
Subarowskii
Doklady Akademii Nauk SSSR, 1952 , vol. 87, p. 759,762
Chem.Abstr., 1954 , p. 164
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Fries; Wolter
Justus Liebigs Annalen der Chemie, 1937 , vol. 527, p. 60,69
参考文献
Fries; Wolter
Justus Liebigs Annalen der Chemie, 1937 , vol. 527, p. 60,69
反应条件
sodium acetate; acetic acid
参考文献
Wheeler
American Chemical Journal, 1895 , vol. 17, p. 699
反应条件
acetic anhydride in water; acetic acid
参考文献
Bo, Yunxin Y.; Chakrabarti, Partha P.; Chen, Ning; Doherty, Elizabeth M.; Fotsch, Christopher H.; Han, Nianhe; Kelly, Michael G.; Liu, Qingyian; Norman, Mark Henry; Ognyanov, Vassil I.; Wang, Xianghong; Zhu, Jiawang
Patent: US2003/195201 A1, 2003 ;
US 20030195201 A1
反应条件
4-(N,N-dimethlyamino)pyridine; N-ethyl-N,N-diisopropylamine in dichloromethane; ethyl acetate
参考文献
Amgen Inc.
Patent: US6878714 B2, 2005 ;
US 6878714 B2
反应条件
in dichloromethane
T=20°C; 24 h; Inert atmosphere;
参考文献
Jepsen, Tue Heesgaard; Larsen, Mogens; Jorgensen, Morten; Nielsen, Mogens Brondsted
Synthesis (Germany), 2013 , vol. 45, # 8 art. no. SS-2013-T0102-OP, p. 1115 - 1120
反应条件
diethyl ether; phosphorus pentachloride
参考文献
Meisenheimer; Zimmermann; v. Kummer
Justus Liebigs Annalen der Chemie, 1926 , vol. 446, p. 225
