反应条件
1: With 4 columns 10cm x 2.5cm with stationary phase Chiralpak AD (Daicel Chemical Industries Ltd.) in methanol T=24.84°C; Resolution of racemate; 2: in methanol T=275°C; P=150.015 Torr; Resolution of racemateCrystallization; 3: in methanol; water T=283°C; Resolution of racemateCrystallization; optical yield given as percent ee;
参考文献
Kaemmerer, Henning; Horvath, Zoltan; Lee, Ju Weon; Kaspereit, Malte; Arnell, Robert; Hedberg, Martin; Herschend, Bjoern; Jones, Matthew J.; Larson, Kerstin; Lorenz, Heike; Seidel-Morgensten, Andreas
Organic Process Research and Development, 2012 , vol. 16, # 2 p. 331 - 342
