(3S,4S)-1-苄基吡咯烷-3,4-二醇合成路线 (共 12 条)
反应条件
sodium tetrahydroborate; iodine in tetrahydrofuran T=20°C;
参考文献
Rejman, Dominik; Kocalka, Petr; Budesinsky, Milos; Pohl, Radek; Rosenberg, Ivan
Tetrahedron, 2007 , vol. 63, # 5 p. 1243 - 1253
反应条件
hydrogenchloride in methanol T=70 - 80°C;
参考文献
Martins, J. Graca; Barrulas, P. Cambeiro; Marques, Carolina S.; Burke, Anthony J.
Synthetic Communications, 2008 , vol. 38, # 9 p. 1365 - 1374
参考文献
Zeeland Chemicals, Inc.
Patent: US6090950 A1, 2000 ;
反应条件
1: 75 percent / Heating 2: 67 percent / NaBH4, BF3*Et2O View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 37, # 13-14 p. 1846 - 1850
参考文献
Yatagai; Yamagishi; Hida
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 823 - 826
反应条件
lithium aluminium tetrahydride in diethyl ether Reflux;
参考文献
Arkivoc, , vol. 2010, # 5 p. 64 - 69
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Hui, Ailing; Zhang, Jintang; Wang, Zhiyong
Synthetic Communications, 2008 , vol. 38, # 14 p. 2374 - 2384
反应条件
1: With hydrogen; palladium 10 on activated carbon in dichloromethane; acetic acid 6 h; 2: With hydrogenchloride in 1,4-dioxane; methanol; toluene
参考文献
WO2008/24725 A1, ;
Page/Page column 123 ;
WO 2008/024725 A1
反应条件
40 Pd(OH)2/C; ammonium formate in methanol 3 h; Reflux;
参考文献
Marradi, Marco; Cicchi, Stefano; Sansone, Francesco; Casnati, Alessandro; Goti, Andrea
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 951 - 957
反应条件
1H-imidazole in N,N-dimethyl-formamide 1.) 0 deg C, 1 h, 2.) r.t., 12 h; Yield given;
参考文献
Cicchi, Stefano; Chierroni, Elisa; Goti, Andrea; Brandi, Alberto; Guerri, Annalisa; Orioli, Pierluigi
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 2 p. 367 - 370