6-氯-1-苯并硫代吡喃-4-酮 1,1-二氧化物合成路线 (共 3 条)
反应条件
dihydrogen peroxide; acetic acid in water 2 h; Reflux;
参考文献
Song, Jiangli; Jones, Lindsay M.; Kumar, G. D. Kishore; Conner, Elizabeth S.; Bayeh, Liela; Chavarria, Gustavo E.; Charlton-Sevcik, Amanda K.; Chen, Shen-En; Chaplin, David J.; Trawick, Mary Lynn; Pinney, Kevin G.
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 6 p. 450 - 453
反应条件
aluminium trichloride; sulfuric acid in carbon disulfide T=25 - 90°C; 4 h;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 19, p. 31 - 44
反应条件
1: 85 percent / AlCl3 / CS2 / 3 h / Ambient temperature 2: H2O2 / acetic acid View Scheme
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 19, p. 31 - 44