N,N-二甲基-2,5-二甲基咪唑-1-磺酰胺合成路线 (共 3 条)
反应条件
n-butyllithium
1.) DME, hexane, -5 deg C, 0.25 h, 2.) room temperature, 12 h; Yield given. Multistep reaction;
参考文献
Chadwick, Derek J.; Ngochindo, Raphael I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 481 - 486
反应条件
n-butyllithium
1.) DME, hexane, -5 deg C, 0.25 h, 2.) -78 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Chadwick, Derek J.; Ngochindo, Raphael I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 481 - 486
反应条件
n-butyllithium
1.) DME, hexane, -5 deg C, 0.25 h, 2.) -78 deg C, 0.5 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Chadwick, Derek J.; Ngochindo, Raphael I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 481 - 486