2-氯-3-溴-5-(羟甲基)吡啶合成路线 (共 2 条)
反应条件
Dess-Martin periodane in dichloromethane
T=0°C; 0.25 h;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GmbH
Patent: WO2009/18656 A1, 2009 ;
Location in patent: Page/Page column 94 ;
反应条件
With thionyl chloride in dichloromethane T=25°C; 5 h; Show Experimental Procedure
参考文献
Zhu, Yuanming; Loso, Michael R.; Nugent, Benjamin M.; Huang, Jim X.; Rogers, Richard B. Patent: US2008/108667 A1, 2008 ; Location in patent: Page/Page column 12 ;