1-(3-甲氧基苄基)-2-硫脲合成路线 （共 3 条）
反应条件
ammonia in dichloromethane
T=0°C; 3.5 h;
参考文献
Goodyer, Claire L. M.; Chinje, Edwin C.; Jaffar, Mohammed; Stratford, Ian J.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 19 p. 4189 - 4206
反应条件
1: 40 percent / CaCO3 / H2O; CHCl3 / 16 h / 20 °C
2: 99 percent / NH3 / CH2Cl2 / 3.5 h / 0 °C
View Scheme
参考文献
Goodyer, Claire L. M.; Chinje, Edwin C.; Jaffar, Mohammed; Stratford, Ian J.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 19 p. 4189 - 4206
反应条件
2: aqueous KOH / nachfolgendes Behandeln mit Chlorokohlensaeure-aethylester und wss. KOH
3: water; NH3
View Scheme
参考文献
Ettlinger; Lundeen
Journal of the American Chemical Society, 1956 , vol. 78, p. 1952
