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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
90584-39-7
合成路线
（共 10 条）
252756-32-4
→
反应条件
90584-39-7
反应条件
lithium hydroxide hydrate in tetrahydrofuran; methanol; water T=20°C; 4 h;
参考文献
Chiang, Chih-Hsiang; Ramu, Ravirala; Tu, Yi-Jung; Yang, Chung-Ling; Ng, Kok Yaoh; Luo, Wen-I; Chen, Charles H.; Lu, Yu-Ying; Liu, Chen-Lun; Yu, Steve S.-F.
Chemistry - A European Journal, 2013 , vol. 19, # 41 p. 13680 - 13691
111-81-9
10-烯酸甲酯
→
反应条件
90584-39-7
反应条件
1.1: 95 percent / Raney Ni (W-2) / methanol / 20 h / 80 °C 2.1: 94 percent / Zn; NiCl2*6H2O / tetrahydrofuran; H2O / 3 h / 20 °C 3.1: 99 percent / LiAlH4 / diethyl ether / 5 h / 20 °C 4.1: 99 percent / 48 percent aq. HBr; H2SO4 / 5 h / 135 °C 5.1: Li / diethyl ether / 1 h 5.2: 40 percent / diethyl ether / 20 °C 6.1: 46.4 percent / CrO3; AcOH / 3 h 7.1: 28 percent / Zn; HgCl2; aq. HCl / toluene / 30 h / Heating 8.1: aq. NaOH View Scheme
参考文献
Gu, Chungang; Wysocki, Vicki H.; Harada, Atsuhiro; Takaya, Hiroaki; Kumadaki, Itsumaro
Journal of the American Chemical Society, 1999 , vol. 121, # 45 p. 10554 - 10562
102684-53-7
→
反应条件
90584-39-7
反应条件
1.1: Li / diethyl ether / 1 h 1.2: 40 percent / diethyl ether / 20 °C 2.1: 46.4 percent / CrO3; AcOH / 3 h 3.1: 28 percent / Zn; HgCl2; aq. HCl / toluene / 30 h / Heating 4.1: aq. NaOH View Scheme
参考文献
Gu, Chungang; Wysocki, Vicki H.; Harada, Atsuhiro; Takaya, Hiroaki; Kumadaki, Itsumaro
Journal of the American Chemical Society, 1999 , vol. 121, # 45 p. 10554 - 10562
125081-42-7
→
反应条件
90584-39-7
反应条件
1.1: 94 percent / Zn; NiCl2*6H2O / tetrahydrofuran; H2O / 3 h / 20 °C 2.1: 99 percent / LiAlH4 / diethyl ether / 5 h / 20 °C 3.1: 99 percent / 48 percent aq. HBr; H2SO4 / 5 h / 135 °C 4.1: Li / diethyl ether / 1 h 4.2: 40 percent / diethyl ether / 20 °C 5.1: 46.4 percent / CrO3; AcOH / 3 h 6.1: 28 percent / Zn; HgCl2; aq. HCl / toluene / 30 h / Heating 7.1: aq. NaOH View Scheme
参考文献
Gu, Chungang; Wysocki, Vicki H.; Harada, Atsuhiro; Takaya, Hiroaki; Kumadaki, Itsumaro
Journal of the American Chemical Society, 1999 , vol. 121, # 45 p. 10554 - 10562
20208-17-7
→
反应条件
90584-39-7
反应条件
1.1: 99 percent / 48 percent aq. HBr; H2SO4 / 5 h / 135 °C 2.1: Li / diethyl ether / 1 h 2.2: 40 percent / diethyl ether / 20 °C 3.1: 46.4 percent / CrO3; AcOH / 3 h 4.1: 28 percent / Zn; HgCl2; aq. HCl / toluene / 30 h / Heating 5.1: aq. NaOH View Scheme
参考文献
Gu, Chungang; Wysocki, Vicki H.; Harada, Atsuhiro; Takaya, Hiroaki; Kumadaki, Itsumaro
Journal of the American Chemical Society, 1999 , vol. 121, # 45 p. 10554 - 10562
188560-98-7
→
反应条件
90584-39-7
反应条件
1: 46.4 percent / CrO3; AcOH / 3 h 2: 28 percent / Zn; HgCl2; aq. HCl / toluene / 30 h / Heating 3: aq. NaOH View Scheme
参考文献
Gu, Chungang; Wysocki, Vicki H.; Harada, Atsuhiro; Takaya, Hiroaki; Kumadaki, Itsumaro
Journal of the American Chemical Society, 1999 , vol. 121, # 45 p. 10554 - 10562
188561-00-4
→
反应条件
90584-39-7
反应条件
1: 28 percent / Zn; HgCl2; aq. HCl / toluene / 30 h / Heating 2: aq. NaOH View Scheme
参考文献
Gu, Chungang; Wysocki, Vicki H.; Harada, Atsuhiro; Takaya, Hiroaki; Kumadaki, Itsumaro
Journal of the American Chemical Society, 1999 , vol. 121, # 45 p. 10554 - 10562
408-34-4
→
反应条件
90584-39-7
反应条件
sodium hydroxide Hydrolysis;
参考文献
Gu, Chungang; Wysocki, Vicki H.; Harada, Atsuhiro; Takaya, Hiroaki; Kumadaki, Itsumaro
Journal of the American Chemical Society, 1999 , vol. 121, # 45 p. 10554 - 10562
112-38-9
10-十一烯酸
+
76-05-1
三氟乙酸
→
反应条件
90584-39-7
反应条件
hydrogen; palladium on activated charcoal 1) acetone, water, 24 h, 2) glacial acetic acid; Yield given. Multistep reaction. Further byproducts given;
参考文献
Muller, Norbert
Journal of Organic Chemistry, 1984 , vol. 49, # 15 p. 2826 - 2827
1344711-01-8
→
反应条件
90584-39-7
反应条件
1: palladium 10 on activated carbon; hydrogen / methanol / 12 h / 20 °C 2: lithium hydroxide hydrate / water; tetrahydrofuran; methanol / 4 h / 20 °C View Scheme
参考文献
Chiang, Chih-Hsiang; Ramu, Ravirala; Tu, Yi-Jung; Yang, Chung-Ling; Ng, Kok Yaoh; Luo, Wen-I; Chen, Charles H.; Lu, Yu-Ying; Liu, Chen-Lun; Yu, Steve S.-F.
Chemistry - A European Journal, 2013 , vol. 19, # 41 p. 13680 - 13691
