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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
905966-40-7
合成路线
（共 26 条）
905966-40-7
+
106-38-7
对溴甲苯
→
反应条件
49742-56-5
4’-甲基[1,1’-联苯]-4-甲酸甲酯
反应条件
potassium phosphate; NiCl2(dppe); 1,2-bis-(diphenylphosphino)ethane in 1,4-dioxane T=110°C; Suzuki-Miyaura cross-coupling; 18 h; Inert atmosphere;
参考文献
Rosen, Brad M.; Huang, Chenghong; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 12 p. 2597 - 2600
905966-40-7
+
138373-10-1
→
反应条件
89900-95-8
4-氰基-[1,1-联苯]-4-羧酸甲酯
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 48 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
905966-40-7
+
1126-46-1
对氯苯甲酸甲酯
→
反应条件
792-74-5
联苯-4,4-二羧酸二甲酯
反应条件
palladium diacetate; cesium fluoride; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane T=25°C; Inert atmosphere;
参考文献
Wilson, Daniela A.; Wilson, Christopher J.; Rosen, Brad M.; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 21 p. 4879 - 4882
905966-40-7
+
51207-43-3
→
反应条件
792-74-5
联苯-4,4-二羧酸二甲酯
反应条件
potassium phosphate; Ni(COD)2; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 8 h; Inert atmosphere;
参考文献
THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA
Patent: WO2009/137322 A2, 2009 ;
Location in patent: Page/Page column 21; 29 ;
905966-40-7
+
619-42-1
对溴苯甲酸甲酯
→
反应条件
792-74-5
联苯-4,4-二羧酸二甲酯
反应条件
potassium phosphate; NiCl2(dppe); 1,2-bis-(diphenylphosphino)ethane in 1,4-dioxane T=110°C; Suzuki-Miyaura cross-coupling; 18 h; Inert atmosphere;
参考文献
Rosen, Brad M.; Huang, Chenghong; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 12 p. 2597 - 2600
905966-40-7
+
161497-18-3
→
反应条件
792-74-5
联苯-4,4-二羧酸二甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 4 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
905966-40-7
+
338396-06-8
→
反应条件
792-74-5
联苯-4,4-二羧酸二甲酯
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
905966-40-7
+
1077-02-7
→
反应条件
89900-94-7
3’-甲基-[1,1’-联苯]-4-甲酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 6 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
905966-40-7
→
反应条件
55676-77-2
[1,1’-联苯]-2,4’-二甲酸二乙酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
905966-40-7
+
95667-98-4
→
反应条件
55676-77-2
[1,1’-联苯]-2,4’-二甲酸二乙酯
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
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