9-甲基-9H-咔唑-3-磺酰氯合成路线 （共 2 条）
反应条件
phosphorus pentachloride; trichlorophosphate
T=90°C; 2 h;
参考文献
Hu, Laixing; Li, Zhuo-rong; Wang, Yue-ming; Wu, Yanbin; Jiang, Jian-Dong; Boykin, David W.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 5 p. 1193 - 1196
反应条件
1: 92 percent / ClSO3H / CH2Cl2 / 2 h / -5 °C
2: 64 percent / POCl3; PCl5 / 2 h / 90 °C
View Scheme
参考文献
Hu, Laixing; Li, Zhuo-rong; Wang, Yue-ming; Wu, Yanbin; Jiang, Jian-Dong; Boykin, David W.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 5 p. 1193 - 1196
