3-碘-1H-吲唑-6-甲腈合成路线 (共 2 条)
反应条件
potassium hydroxide; iodine in N,N-dimethyl-formamide
T=23°C; 5 h;
参考文献
MERCK and CO., INC.
Patent: WO2006/86255 A2, 2006 ;
Location in patent: Page/Page column 39-40 ;
WO 2006/086255 A2
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; triethylamine in toluene
T=80°C; P=750.075 Torr; Autoclave;
参考文献
Buchstaller, Hans-Peter; Wilkinson, Kai; Burek, Kasimir; Nisar, Yasmin
Synthesis, 2011 , # 19 art. no. T48411SS, p. 3089 - 3098