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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
90633-61-7
合成路线
（共 11 条）
106708-08-1
→
反应条件
90633-61-7
+
89268-74-6
反应条件
(-)-2,3-O-isopropylidene-2,3-dihydroxy-1,4-bis(diphenylphosphanyl)butane; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=0°C; 14 h; Yields of byproduct given;
参考文献
Hiroi, Kunio; Makino, Kunitaka
Chemistry Letters, 1986 , p. 617 - 620
112473-05-9
→
反应条件
90633-61-7
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=25°C; 12 h;
参考文献
Kobayashi, Toshifumi; Tanaka, Yuhji; Ohtani, Takashi; Kinoshita, Hideki; Inomata, Katsuhiko; Kotake, Hiroshi
Chemistry Letters, 1987 , p. 1209 - 1212
111895-50-2
→
反应条件
90633-61-7
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=25°C; 12 h;
参考文献
Kobayashi, Toshifumi; Tanaka, Yuhji; Ohtani, Takashi; Kinoshita, Hideki; Inomata, Katsuhiko; Kotake, Hiroshi
Chemistry Letters, 1987 , p. 1209 - 1212
3913-80-2
(E)-辛-2-烯基乙酸酯
+
824-79-3
对甲苯亚磺酸钠
→
反应条件
90633-61-7
+
89268-74-6
反应条件
(-)-2,3-O-isopropylidene-2,3-dihydroxy-1,4-bis(diphenylphosphanyl)butane; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 6 h; Ambient temperature; Yields of byproduct given;
参考文献
Hiroi, Kunio; Makino, Kunitaka
Chemistry Letters, 1986 , p. 617 - 620
824-79-3
对甲苯亚磺酸钠
→
反应条件
90633-61-7
反应条件
1: 92 percent / I2 / H2O; ethyl acetate / 24 h / Ambient temperature 2: 96 percent / hydrogen, sodium acetate / Pd-C, quinoline / methanol / 2.5 h / Ambient temperature 3: 96 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / acetonitrile / 12 h / 25 °C View Scheme
参考文献
Kobayashi, Toshifumi; Tanaka, Yuhji; Ohtani, Takashi; Kinoshita, Hideki; Inomata, Katsuhiko; Kotake, Hiroshi
Chemistry Letters, 1987 , p. 1209 - 1212
629-05-0
1-辛炔
→
反应条件
90633-61-7
反应条件
1: 92 percent / I2 / H2O; ethyl acetate / 24 h / Ambient temperature 2: 96 percent / hydrogen, sodium acetate / Pd-C, quinoline / methanol / 2.5 h / Ambient temperature 3: 96 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / acetonitrile / 12 h / 25 °C View Scheme
参考文献
Kobayashi, Toshifumi; Tanaka, Yuhji; Ohtani, Takashi; Kinoshita, Hideki; Inomata, Katsuhiko; Kotake, Hiroshi
Chemistry Letters, 1987 , p. 1209 - 1212
28995-78-0
→
反应条件
90633-61-7
反应条件
1: 96 percent / hydrogen, sodium acetate / Pd-C, quinoline / methanol / 2.5 h / Ambient temperature 2: 96 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / acetonitrile / 12 h / 25 °C View Scheme
参考文献
Kobayashi, Toshifumi; Tanaka, Yuhji; Ohtani, Takashi; Kinoshita, Hideki; Inomata, Katsuhiko; Kotake, Hiroshi
Chemistry Letters, 1987 , p. 1209 - 1212
119365-13-8
→
反应条件
90633-61-7
+
79243-02-0
反应条件
triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 17 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Hiroi, Kunio; Kitayama, Ryuichi; Sato, Shuko
Journal of the Chemical Society, Chemical Communications, 1984 , # 5 p. 303 - 305
106708-08-1
→
反应条件
90633-61-7
+
79243-02-0
反应条件
triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 15.5 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Hiroi, Kunio; Kitayama, Ryuichi; Sato, Shuko
Journal of the Chemical Society, Chemical Communications, 1984 , # 5 p. 303 - 305
111-66-0
1-辛烯
→
反应条件
90633-61-7
反应条件
1: I2 / H2O; ethyl acetate / 2 h / Ambient temperature 2: acetonitrile / Ambient temperature 3: MCPBA, Na2CO3 / CH2Cl2 / Ambient temperature 4: 97 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / acetonitrile / 12 h / 25 °C View Scheme
参考文献
Kobayashi, Toshifumi; Tanaka, Yuhji; Ohtani, Takashi; Kinoshita, Hideki; Inomata, Katsuhiko; Kotake, Hiroshi
Chemistry Letters, 1987 , p. 1209 - 1212
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