1-(4-甲氧基苯基)乙胺盐酸盐合成路线 （共 5 条）
反应条件
hydrogenchloride; hydrogen; palladium 10 on activated carbon in ethanol; water
P=760.051 Torr;
参考文献
INSTITUTE OF MATERIA MEDICA, CHINESE ACADEMY OF MEDICAL SCIENCES
Patent: EP2511283 A1, 2012 ;
Location in patent: Page/Page column 63 ;
反应条件
hydrogenchloride in diethyl ether
T=0°C; 0.5 h;
参考文献
Guy, Alain; Lemor, Alain; Doussot, Joel; Lemaire, Marc
Synthesis, 1988 , # 11 p. 900 - 902
反应条件
1: H2 / Pd-BaSO4 (5percent) / ethanol / 4 h / 760 Torr / Ambient temperature
2: HCl / diethyl ether / 0.5 h / 0 °C
View Scheme
参考文献
Guy, Alain; Lemor, Alain; Doussot, Joel; Lemaire, Marc
Synthesis, 1988 , # 11 p. 900 - 902
反应条件
1: Me3SiN3, DDQ / CHCl3 / 51 h / Ambient temperature
2: H2 / Pd-BaSO4 (5percent) / ethanol / 4 h / 760 Torr / Ambient temperature
3: HCl / diethyl ether / 0.5 h / 0 °C
View Scheme
参考文献
Guy, Alain; Lemor, Alain; Doussot, Joel; Lemaire, Marc
Synthesis, 1988 , # 11 p. 900 - 902
反应条件
1: hydroxylamine hydrochloride; sodium acetate / ethanol / 6 h / 60 °C
2: hydrogenchloride; hydrogen / palladium 10 on activated carbon / ethanol; water / 760.05 Torr
View Scheme
参考文献
INSTITUTE OF MATERIA MEDICA, CHINESE ACADEMY OF MEDICAL SCIENCES
Patent: EP2511283 A1, 2012 ;
