1-[[(1,1-二甲基乙基)二甲基甲硅烷基]氧基]-环丙烷羧醛合成路线 （共 3 条）
反应条件
oxalyl dichloride; dimethyl sulfoxide in tetrahydrofuran
T=-78°C; 0.5 h;
参考文献
Nemoto, Hideo; Ishibashi, Hiroki; Mori, Masahiko; Fujita, Shigekazu; Fukumoto, Keiichiro
Heterocycles, 1990 , vol. 31, # 7 p. 1237 - 1240
反应条件
1: imidazole / dimethylformamide
2: 1.) DIBAH; 2.) oxalyl chloride, dimethylsulfoxide / 1.) toluene, -70 deg C
View Scheme
参考文献
Barnier, J. P.; Salauen, J.
Tetrahedron Letters, 1984 , vol. 25, # 12 p. 1273 - 1276
反应条件
oxalyl dichloride; diisobutylaluminium hydride; dimethyl sulfoxide
1.) toluene, -70 deg C; Yield given. Multistep reaction;
参考文献
Barnier, J. P.; Salauen, J.
Tetrahedron Letters, 1984 , vol. 25, # 12 p. 1273 - 1276
