1: in tetrahydrofuran
T=0°C; 0.166667 h; Inert atmosphereSealed tube;
2: With tetrabutyl ammonium fluoride in tetrahydrofuran
T=0 - 20°C; Inert atmosphereSealed tube;
3: With tetrabutyl ammonium fluoride; water in tetrahydrofuran
T=0 - 20°C; Inert atmosphereSealed tube;
参考文献
Kelly, Christopher B.; Mercadante, Michael A.; Hamlin, Trevor A.; Fletcher, Madison H.; Leadbeater, Nicholas E.
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8131 - 8141
1.1: tetrahydrofuran / 0.17 h / 0 °C / |Inert atmosphere; |Sealed tube
1.2: 0 - 20 °C / |Inert atmosphere; |Sealed tube
1.3: 0 - 20 °C / |Inert atmosphere; |Sealed tube
2.1: oxoammonium salt; 2,6-dimethylpyridine / dichloromethane / 20 °C / |Sealed tube
View Scheme
参考文献
Kelly, Christopher B.; Mercadante, Michael A.; Hamlin, Trevor A.; Fletcher, Madison H.; Leadbeater, Nicholas E.
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8131 - 8141
