2-(1,3-二氧杂烷-2-基)乙醛合成路线 （共 4 条）
反应条件
oxalic acid; silica gel in tetrahydrofuran; 1,2-dichloro-ethane
T=80°C; 8 h;
参考文献
Shi-Qi, Peng; Winterfeldt, Ekkehard
Liebigs Annalen der Chemie, 1989 , p. 1045 - 1047
反应条件
pyridinium chlorochromate in dichloromethane
参考文献
Baxter, Anthony D.; Binns, Falmai; Javed, Tariq; Roberts, Stanley M.; Sadler, Peter; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 889 - 900
反应条件
diisobutylaluminium hydride in tetrahydrofuran; dichloromethane
T=-78°C; 6 h;
参考文献
Ducho, Christian; Hamed, Refaat B.; Batchelar, Edward T.; Sorensen, John L.; Odell, Barbara; Schofield, Christopher J.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 13 p. 2770 - 2779
反应条件
1: 89 percent / Na / liquid ammonia; tetrahydrofuran
2: 74 percent / PCC / CH2Cl2
View Scheme
参考文献
Baxter, Anthony D.; Binns, Falmai; Javed, Tariq; Roberts, Stanley M.; Sadler, Peter; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 889 - 900
