2-溴甲基-5-硝基苯甲酸甲酯合成路线 (共 7 条)
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 34 h; Reflux;
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS; PURDUE RESEARCH FOUNDATION
Patent: US2011/269834 A1, 2011 ;
Location in patent: Page/Page column 29 ;
反应条件
dibenzoyl peroxide in tetrachloromethane; water
参考文献
EP514133 A1, ;
EP 0514133 A1
反应条件
1: AcCl / Heating 2: N-bromosuccinimide (NBS), benzoyl peroxide / CCl4 / 20 h / Heating View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 26, # 7 p. 699 - 707
反应条件
1: sulfuric acid 2: sulfuric acid; nitric acid 3: N-bromosuccinmide; dibenzoyl peroxide; tetrachloromethane View Scheme
参考文献
Inorganic Chemistry, , vol. 53, # 6 p. 2932 - 2942
反应条件
1: sulfuric acid; nitric acid 2: N-bromosuccinmide; dibenzoyl peroxide; tetrachloromethane View Scheme
参考文献
Inorganic Chemistry, , vol. 53, # 6 p. 2932 - 2942
反应条件
1: NaOH, tricaprylmethylammonium chloride / CH2Cl2; H2O / 5 h / Ambient temperature 2: 82 percent / aq. 4 N KOH / methanol / 4 h / Ambient temperature View Scheme
参考文献
Wakselman; Mazaleyrat; Xie; Montagne; Vilain; Reboud-Ravaux
European Journal of Medicinal Chemistry, 1991 , vol. 26, # 7 p. 699 - 707
反应条件
ammonia in methanol 2 h; Reflux;
参考文献
Fu, Liqiang; Liu, Xin; Ling, Chenyu; Cheng, Jianjun; Guo, Xingsheng; He, Huili; Ding, Shi; Yang, Yushe
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 2 p. 814 - 819