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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
90769-34-9
合成路线
（共 6 条）
1903-22-6
2-亚环戊基乙酸乙酯
→
反应条件
90769-34-9
反应条件
1: H2 / 5percent Pd/C / ethanol / 760 Torr 2: LiAlH4 / tetrahydrofuran 3: PBr3 / diethyl ether; diethyl ether / 16 h / Ambient temperature 4: 94.7 percent / dimethylsulfoxide 5: 78 percent / CF3COOH View Scheme
参考文献
Yokohama; Miwa; Aibara; Fujiwara; Matsumoto; Nakayama; Iwamoto; Mori; Moroi; Tsukada; Isoda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2391 - 2398
120-92-3
环戊酮
→
反应条件
90769-34-9
反应条件
1: NaH / benzene 2: H2 / 5percent Pd/C / ethanol / 760 Torr 3: LiAlH4 / tetrahydrofuran 4: PBr3 / diethyl ether; diethyl ether / 16 h / Ambient temperature 5: 94.7 percent / dimethylsulfoxide 6: 78 percent / CF3COOH View Scheme
参考文献
Yokohama; Miwa; Aibara; Fujiwara; Matsumoto; Nakayama; Iwamoto; Mori; Moroi; Tsukada; Isoda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2391 - 2398
1123-04-2
+
79-19-6
氨基硫脲
→
反应条件
90769-34-9
反应条件
trifluoroacetic acid
参考文献
Yokohama; Miwa; Aibara; Fujiwara; Matsumoto; Nakayama; Iwamoto; Mori; Moroi; Tsukada; Isoda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2391 - 2398
18928-94-4
(2-溴乙基)环戊烷
→
反应条件
90769-34-9
反应条件
1: 94.7 percent / dimethylsulfoxide 2: 78 percent / CF3COOH View Scheme
参考文献
Yokohama; Miwa; Aibara; Fujiwara; Matsumoto; Nakayama; Iwamoto; Mori; Moroi; Tsukada; Isoda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2391 - 2398
18322-54-8
环戊基乙酸乙酯
→
反应条件
90769-34-9
反应条件
1: LiAlH4 / tetrahydrofuran 2: PBr3 / diethyl ether; diethyl ether / 16 h / Ambient temperature 3: 94.7 percent / dimethylsulfoxide 4: 78 percent / CF3COOH View Scheme
参考文献
Yokohama; Miwa; Aibara; Fujiwara; Matsumoto; Nakayama; Iwamoto; Mori; Moroi; Tsukada; Isoda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2391 - 2398
766-00-7
2-环戊基乙醇
→
反应条件
90769-34-9
反应条件
1: PBr3 / diethyl ether; diethyl ether / 16 h / Ambient temperature 2: 94.7 percent / dimethylsulfoxide 3: 78 percent / CF3COOH View Scheme
参考文献
Yokohama; Miwa; Aibara; Fujiwara; Matsumoto; Nakayama; Iwamoto; Mori; Moroi; Tsukada; Isoda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2391 - 2398
