4,4’-二羟基-2,2’-联吡啶合成路线 （共 3 条）
反应条件
phosphorus tribromide in N,N-dimethyl-formamide T=20°C; 1 h; Inert atmosphere;
参考文献
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, , vol. 94, p. 340 - 345
反应条件
hydrogen bromide; acetic acid in water
47 h; Inert atmosphereReflux;
参考文献
Willemsen, Jorgen S.; Van Hest, Jan C.M.; Rutjes, Floris P.J.T.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 960 - 965
反应条件
1: 34 percent / Pd(PPh3)4 / xylene / 12 h / Heating
2: 87 percent / Pyridiniumchlorid / 4 h / Heating
View Scheme
参考文献
Dehmlow, Eckehard V.; Sleegers, Arthur
Liebigs Annalen der Chemie, 1992 , # 9 p. 953 - 960
