(6,7-二甲氧基-1H-吲哚-3-基)-乙酸甲酯合成路线 (共 4 条)
反应条件
triethylamine; palladium diacetate; tris-(o-tolyl)phosphine in acetonitrile
Heck cyclization; 3 h; Heating;
参考文献
Mejia-Oneto, Jose M.; Padwa, Albert
Helvetica Chimica Acta, 2008 , vol. 91, # 2 p. 285 - 302
反应条件
1: 47 percent / NaHCO3 / acetone; H2O / 3 h / Heating
2: 90 percent / triethylamine / palladium(II) acetate; tri-o-tolylphosphine / acetonitrile / 3 h / Heating
View Scheme
参考文献
Mejia-Oneto, Jose M.; Padwa, Albert
Organic Letters, 2006 , vol. 8, # 15 p. 3275 - 3278
反应条件
1: 47 percent / NaHCO3 / acetone; H2O / 3 h / Heating
2: 90 percent / triethylamine / palladium(II) acetate; tri-o-tolylphosphine / acetonitrile / 3 h / Heating
View Scheme
参考文献
Mejia-Oneto, Jose M.; Padwa, Albert
Organic Letters, 2006 , vol. 8, # 15 p. 3275 - 3278
反应条件
1: 73 percent / iodine monochloride; Na2CO3 / diethyl ether; H2O / 2 h
2: 47 percent / NaHCO3 / acetone; H2O / 3 h / Heating
3: 90 percent / triethylamine / palladium(II) acetate; tri-o-tolylphosphine / acetonitrile / 3 h / Heating
View Scheme
参考文献
Mejia-Oneto, Jose M.; Padwa, Albert
Organic Letters, 2006 , vol. 8, # 15 p. 3275 - 3278