908093-98-1合成路线 （共 442 条）
反应条件
T=24.9°C; Irradiationlaser flash photolysis;
参考文献
Alberti, A.; Griller, D.; Nazran, A. S.; Pedulli, G. F.
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 3024 - 3028
反应条件
copper(l) iodide; lithium tert-butylate in toluene
T=110°C; 0.833333 h; Inert atmosphere;
参考文献
Zhao, Xia; Wu, Guojiao; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 10 p. 3296 - 3299
反应条件
1: H2SO4; benzene
2: ethanolic KOH
View Scheme
参考文献
Curtin; Leskowitz
Journal of the American Chemical Society, 1951 , vol. 73, p. 2630,2632
参考文献
Benati, Luisa; Montevecchi, Pier Carlo; Spagnolo, Piero; Tundo, Antonio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1544 - 1548
反应条件
in chlorobenzene
T=80°C; under oxygen; Product distribution;
参考文献
Benati, Luisa; Montevecchi, Pier Carlo; Spagnolo, Piero
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1437 - 1442
反应条件
cyclohexane
Irradiation.mit UV-Licht;
参考文献
Kirmse et al.
Justus Liebigs Annalen der Chemie, 1958 , vol. 614, p. 19,30
参考文献
Perusquia-Hernandez, Carolina; Lara-Issasi, Gonzalo R.; Frontana-Uribe, Bernardo A.; Cuevas-Yanez, Erick
Tetrahedron Letters, 2013 , vol. 54, # 25 p. 3302 - 3305
反应条件
1: (2S)-8-[(1R)-1,3-diphenylpropyl]-5,7,3',4'-tetramethoxyflavan With ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile
T=20°C; Oxidation; 2 h;
2: diphenyldiazo-methane in tetrahydrofuran; methanol
T=20°C; Alkylation; 65 h;
参考文献
Kozikowski, Alan P.; Tueckmantel, Werner; George, Clifford
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5371 - 5381
反应条件
1: (S)-2-(3,4-Dimethoxy-phenyl)-8-(1,3-diphenyl-propyl)-5,7-dimethoxy-chroman With ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile
T=20°C; Oxidation; 2 h;
2: diphenyldiazo-methane in tetrahydrofuran; methanol
T=20°C; Alkylation; 19.1 h; Further byproducts given;
参考文献
Kozikowski, Alan P.; Tueckmantel, Werner; George, Clifford
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5371 - 5381
反应条件
in diethyl ether; dichloromethane; pentane
T=-78 - 20°C;
参考文献
Javed, Muhammad I.; Brewer, Matthias
Organic Letters, 2007 , vol. 9, # 9 p. 1789 - 1792
