908093-98-1合成路线 （共 442 条）
反应条件
diethyl ether
unter Lichtabschluss;
参考文献
Schoenberg; Schuetz; Peter
Chemische Berichte, 1929 , vol. 62, p. 1667
参考文献
Busch; Knoll
Chemische Berichte, 1927 , vol. 60, p. 2254
反应条件
in tetrahydrofuran
T=-78°C;
参考文献
Okuma, Kentaro; Kojima, Kazuki; Ohta, Hiroshi
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 80, # 1-4 p. 259 - 262
反应条件
in acetone
T=20°C; Alkylation; 2 h;
参考文献
Sandanayaka; Yang
Organic letters, 2000 , vol. 2, # 20 p. 3087 - 3090
反应条件
1: acetone / 0 - 20 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C
View Scheme
参考文献
Nottingham, Micheal; Bethel, Christopher R.; Pagadala, Sundar Ram Reddy; Harry, Emily; Pinto, Abishai; Lemons, Zachary A.; Drawz, Sarah M.; Akker, Focco Van Den; Carey, Paul R.; Bonomo, Robert A.; Buynak, John D.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 1 p. 387 - 393
参考文献
Arbuzov, B. A.; Dianova, E. N.; Zabotina, E. Ya.; Chadaeva, N. A.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 4 p. 835 - 838,733 - 736
参考文献
Arbuzov, B. A.; Dianova, E. N.; Chadaeva, N. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 6 p. 1280
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 6 p. 1432 - 1433
参考文献
Merck and Co.Inc.
Patent: US2595405 , 1949 ;
反应条件
in diethyl ether
T=25°C; 8 h; Irradiation;
参考文献
Oku, Akira; Yokoyama, Taka-aki; Harada, Toshiro
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5333 - 5337
反应条件
1: 70 percent / diethyl ether / 8 h / 25 °C / Irradiation
2: 92 percent / 35percent HCl / H2O; dioxane / 1.5 h / 90 °C
View Scheme
参考文献
Oku, Akira; Yokoyama, Taka-aki; Harada, Toshiro
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5333 - 5337
