908094-04-2合成路线 (共 238 条)
反应条件
1: 92 percent / diethyl ether / -15 °C
2: 2.) NaOH/MeOH / 1.) toluene, 90 deg C; 2.) 25 deg C
View Scheme
参考文献
Suzuki, M.; Gooch, E. E.; Stammer, C. H.
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3839 - 3840
反应条件
T=15°C; Irradiationvariation of temperature, matrix effect, further chloro compound; Product distribution;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Chemistry Letters, 1980 , p. 293 - 296
反应条件
in diethyl ether
Ambient temperature;
参考文献
Maerkl, Gottfried; Troetsch, Irene
Angewandte Chemie, 1984 , vol. 96, # 11 p. 899 - 901
反应条件
Ambient temperatureIrradiation;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Journal of the American Chemical Society, 1982 , vol. 104, # 11 p. 3156 - 3162
反应条件
isopropyl alcohol
T=70°C; Yield given. Title compound not separated from byproducts;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Journal of the American Chemical Society, 1982 , vol. 104, # 4 p. 1047 - 1050
反应条件
ethyl vinyl ether
T=70°C; Yields of byproduct given;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Journal of the American Chemical Society, 1982 , vol. 104, # 4 p. 1047 - 1050
反应条件
isopropyl alcohol
T=25°C; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Journal of the American Chemical Society, 1982 , vol. 104, # 4 p. 1047 - 1050
反应条件
methanol in 1,4-dioxane
T=10°C; Irradiation; Yield given. Yields of byproduct given;
参考文献
Tomoika, H.; Ozaki, Y.; Izawa, Y
Tetrahedron, 1985 , vol. 41, # 21 p. 4987 - 4994
反应条件
T=-196°C; (photolysis);
参考文献
Tomioka,H. et al.
Journal of the American Chemical Society, 1979 , vol. 101, p. 6009 - 6012
反应条件
in solid matrix
T=-110°C; Irradiationtemperature dependence of product distributions, added sensitizer; Product distribution;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Journal of the American Chemical Society, 1982 , vol. 104, # 11 p. 3156 - 3162