908094-04-2合成路线 (共 238 条)
参考文献
Yates; Shapiro
Journal of Organic Chemistry, 1958 , vol. 23, p. 759
反应条件
1: petroleum ether; diethyl ether; anhydrous HF / -70 °C 2: diethyl ether View Scheme
参考文献
Chemische Berichte, , vol. 74, p. 1474,1488
参考文献
Yates; Shapiro
Journal of Organic Chemistry, 1958 , vol. 23, p. 759
反应条件
scandium tris(trifluoromethanesulfonate) in toluene T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Wommack, Andrew J.; Moebius, David C.; Travis, Austin L.; Kingsbury, Jason S.
Organic Letters, 2009 , vol. 11, # 15 p. 3202 - 3205
反应条件
zinc(II) iodide in diethyl ether 2 h; Ambient temperature;
参考文献
Bartnik, R.; Mloston, G.
Acta Chimica Academiae Scientiarum Hungaricae, 1981 , vol. 106, # 4 p. 309 - 312
参考文献
Wittig,G.; Schlosser,M.
Tetrahedron, 1962 , vol. 18, p. 1023 - 1028
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene T=25°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Oshima, Takumi; Nagai, Toshikazu
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3865 - 3870
参考文献
Jones; Kenner
Journal of the Chemical Society, 1933 , p. 363,366
反应条件
tetrafluoroboric acid in dichloromethane T=0°C; 0.25 h; Title compound not separated from byproducts;
参考文献
Israel Journal of Chemistry, , vol. 31, # 3 p. 215 - 222
反应条件
in diethyl ether; pentane T=-20°C; 4 h; Further byproducts given. Yields of byproduct given;
参考文献
Journal of Chemical Research, Miniprint, , # 6 p. 1701 - 1708